Henley's Twentieth Century Formulas, Recipes and Processes. Various

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      This air bath is employed in cases in which, upon drying or heating substances, acid vapors arise because the walls of the bath are not attacked by them. For the production of the drying apparatus take a flask with the bottom burst off or a bell jar tubulated above. This is placed either upon a sand bath or upon asbestos paper, previously laid upon a piece of sheet iron. The sand bath or the sheet iron is put on a tripod, so that it can be heated by means of a burner placed underneath. The substance to be dried is placed in a glass or porcelain dish, which is put under the bell jar, and if desired the drying dish may be hung on the tripod. For regulating the temperature the tubulure of the jar is closed with a pierced cork, through whose aperture the thermometer is thrust. In order to permit the vapors to escape, the cork is grooved lengthwise along the periphery.

      AIR BUBBLES IN GELATINE: See Gelatine.

      AIR, EXCLUSION OF, FROM SOLUTIONS: See Photography.

AIR-PURIFYING.

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      Ozonatine

      is a fragrant air-purifying preparation consisting of dextrogyrate turpentine oil scented with slight quantities of fragrant oils.

      ALABASTER CLEANING: See Cleaning Preparations and Methods.

      ALBATA METAL: See Alloys.

ALBUMEN IN URINE, DETECTION OF.

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      Patein (Pharm. Zeit.) recommends the following test for albumen in urine: Dissolve 250 grams of citric acid in a sufficient quantity of water, add enough ammonia to neutralize, then 50 grams of alcohol, and finally enough water to make 1 liter. To the acid (or acidulated) urine, one-tenth its volume of the ammonium-citrate solution made as above is added, and the whole heated in the usual manner. The appearance of the faintest turbidity is said to indicate with positive certainty the presence of albumen.

      ALBUMEN PAPER: See Photography.

      ALBUMEN PASTE: See Adhesives.

ALCOHOL

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      After the manuscript of this book was ready for the press, Congress passed the bill which has since become a law, whereby the prohibitive tax on industrial or denatured alcohol is removed. So important is this legislative measure that the Editor has deemed it wise to insert an article on the sources of alcohol and the manufacture of alcohol from farm products. Because the first portion of the book was in type when this step was decided upon, the Editor was compelled to relegate to a later page a monograph which should properly have appeared here. The reader will find the matter on alcohol referred to under the heading {45} “Spirit”; likewise methods of denaturing and a list of denaturants.

      ALCOHOL, DILUTION OF: See Tables.

      Alcohol, Tests For Absolute.

      —The committee for the compilation of the German Arzneibuch established the following tests for the determination of absolute alcohol:

      Absolute alcohol is a clear, colorless, volatile, readily imflammable liquid which burns with a faintly luminous flame. Absolute alcohol has a peculiar odor, a burning taste, and does not affect litmus paper. Boiling point, 78.50. Specific gravity, 0.795 to 0.797. One hundred parts contain 99.7 to 99.4 parts, by volume, or 99.6 to 99.0 parts, by weight, of alcohol.

      Absolute alcohol should have no foreign smell and should mix with water without cloudiness.

      After the admixture of 5 drops of silver-nitrate solution, 10 cubic centimeters of absolute alcohol should not become turbid or colored even on heating.

      A mixture of 10 cubic centimeters of absolute alcohol and 0.2 cubic centimeter of potash lye evaporated down to 1 cubic centimeter should not exhibit an odor of fusel oil after supersaturation with dilute sulphuric acid.

      Five cubic centimeters of sulphuric acid, carefully covered, in a test tube, with a stratum of 5 cubic centimeters of absolute alcohol, should not form a rose-colored zone at the surface of contact, even on standing for some time.

      The red color of a mixture of 10 cubic centimeters of absolute alcohol and 1 cubic centimeter of potassium-permanganate solution should not pass into yellow before 20 minutes.

      Absolute alcohol should not be dyed by hydrogen sulphide water or by aqueous ammonia.

      Five cubic centimeters of absolute alcohol should not leave behind a weighable residue after evaporation on water bath.

      Absolute Alcohol.

      —If gelatine be suspended in ordinary alcohol it will absorb the water, but as it is insoluble in alcohol, that substance will remain behind, and thus nearly absolute alcohol will be obtained without distillation.

      Perfumed Denaturized Alcohol.—

East India lemon oil	1,250 parts
Mirbane oil	1,000 parts
Cassia oil	50 parts
Clove oil	75 parts
Lemon oil	100 parts
Amyl acetate	500 parts
Spirit (95 per cent)	7,000 parts

      Dissolve the oils in the spirit and add the amyl acetate. The mixture serves for destroying the bad odor of denaturized spirit in distilling. Use 50 parts of the perfume per 1,000 parts of spirit.

      Solid Alcohol.

      —I.—Heat 1,000 parts of denaturized alcohol (90 per cent) in a flask of double the capacity on the water bath to about 140° F., and then mix with 28 to 30 parts of well-dried, rasped Venetian soap and 2 parts of gum lac. After repeated shaking, complete dissolution will take place. The solution is put, while still warm, into metallic vessels, closing them up at once and allowing the mixture to cool therein. The admixture of gum lac effects a better preservation and also prevents the evaporation of the alcohol. On lighting the solid spirit the soap remains behind.

      II.—Smaragdine is a trade name for solidified alcohol. It consists of alcohol and gun cotton, colored with malachite green. It appears in the market in the form of small cubes.

      Alcohol In Fermented Beers.

      —Experience has shown that 1/4 pound of sugar to 1 gallon of water yields about 2 per cent of proof spirit, or about 1 per cent of absolute alcohol. Beyond this amount it is not safe to go, if the legal limit is to be observed, yet a ginger beer brewed with 1/4 pound per gallon of sugar would be a very wishy-washy compound, and there is little doubt that a much larger quantity is generally used. The more sugar that is used—up to 1 1/2 or 1 1/4 pounds per gallon—the better the drink will be and the more customers will СКАЧАТЬ