Geophysical Monitoring for Geologic Carbon Storage. Группа авторов

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СКАЧАТЬ rock to scCO₂ has been observed to affect the rock wettability (McCool & Tripp, 2005) and thus scCO₂ invasion, the scCO₂‐saturated case was estimated by interpolating between the CT‐indicated density numbers of the water‐saturated and dry cases based on the relative densities of the water and scCO₂. This approach is generally effective where the spatial scale of the CT noise is smaller than the spatial scale of the features of interest. For CO₂ saturation in a fracture where the spatial scale of noise is larger than the fracture aperture, a segmentation approach was used in which the location of the fracture aperture was determined from the dry set of scans, and computations of differences were performed on those specific locations separately.

      5.2.3. Samples and Test Cases

A series of seismic measurements with X‐ray CT imaging was conducted on two Carbon Tan sandstone core samples (Kocurek Industries, Inc., http://www.kocurekindustries.com/) with various fracture configurations (Table 5.1). The sandstone has a porosity of 16.7% and a matrix permeability of 34.5 md (measured only for the Carbon Tan #2 core. However, similar dry densities of the #1 and #2 cores (2,380 kg/m³ and 2,375 kg/m³, respectively) indicate that the #1 core has a similar porosity. The permeability was measured using the falling‐head permeability test method (e.g., Head, 1982) under unconfined conditions, using tap water at room temperature. The diameter of the cores was 38 mm, and the length varied slightly among the cores, from 98 mm to 101 mm. A single fracture was introduced in each core via extensile splitting (Brazilian loading) either parallel or perpendicular to the core axis.

Table 5.1 Descriptions of test samples with different fracture configurations

Sample	Description	scCO2 injection rate (mL/min)	Configuration
Carbon Tan #1 core	Intact I	Intact core	0.035
	Frac Ia	Mated core‐parallel fracture (no offset)	0.037
	Frac Ib	Sheared core‐parallel fracture; with spacers	0.017
	Frac Ic	Sheared core‐parallel fracture; without spacers (shorter core)	0.027
	Frac Id	Same as Frac Ic sample, but with a vertically oriented fracture	0.043
Carbon Tan #2 core	Intact II	Intact core	0.042
	Frac IIa	Sheared (rotationally offset) core‐perpendicular fracture; with a mylar wrapping	0.023
	Frac IIb	Sheared (rotationally offset) core‐perpendicular fracture	0.020

      Note: The core numbers were redesignated in this paper and can be different from what are seen in the photographs.

      The first core sample (Carbon Tan #1) was tested for: intact state (Intact I); a mated, core‐parallel fracture (Frac Ia); a sheared (linearly displaced) core‐parallel fracture with end spacers (Frac Ib); and a sheared core parallel fracture without end spacers (Frac Ic). The end spacers (thickness 3 mm) in the Frac Ib test, which were coupled to the sample and the metal rods using thin lead foil disks, were made from the same sandstone and were used to apply and maintain a shear offset along the fracture surface. These spacers were later removed, and the protruding sample ends were ground flat for use in the Frac Ic test. These tests were all conducted while the fracture was oriented horizontally. In addition, the same test as Frac Ic was conducted while the fracture was oriented vertically to examine the effect of buoyancy‐controlled scCO₂ migration within the fracture on seismic waves (Frac Id).

      For the second core sample (Carbon Tan #2), tests were conducted for: intact state (Intact II); a sheared (rotational offset) core‐perpendicular fracture with a Mylar wrapping (Frac IIa); and the same sample as Frac IIa without the Mylar wrapping (Frac IIb). Note that for Frac IIa test, scCO₂ followed a preferential flow path along the Mylar sheet, resulting in premature breakthrough across the core. This test can be viewed as a special case where both core‐perpendicular and core‐parallel fractures are present. However, the permeability of this fast‐pass‐providing core‐parallel “fracture” was thought to be small.

      5.2.4. Determination of Elastic Moduli and Attenuation From Measured Resonances

      SHRB measurements determine dynamic Young's modulus E, shear modulus G, and their related attenuations (vibration damping factors) a _E and a _G respectively (given by 1/2Q _E and 1/2Q _G using the seismic quality factors). Note that for anisotropic rock, E is the longitudinal modulus along the core axis, and G is the torsion modulus around the core axis. During an experiment, fundamental‐mode resonances of both longitudinal‐mode vibration and torsional‐mode vibration are measured, using combinations of longitudinal piezoelectric source and the axial accelerometer, and of the torsional source and the tangential accelerometers, respectively. For each resonance, its peak frequency f _c and the half‐power width Δf are measured. From these values, the quality factor of the resonance is obtained by СКАЧАТЬ